Patent · US Active

Catalytic oxidation of polar modifiers in chromatographic mobile phases

US10151733B2 · kind B2 · utility

1Cited by
3References
18Claims
0Family size

Assignee

Inventors

Key dates

Filing dateSep 12, 2014
Grant dateDec 11, 2018
Priority date
Expiry dateNov 13, 2034

Classification

  • Technology area (CPC G)Physics
  • CPC primaryG01N2030/8435
  • WIPO fieldMeasurement
  • WIPO sectorInstruments

Abstract

The present disclosure relates to an oxidizer, and related methods, for oxidizing polar modifiers in chromatographic mobile phases. The oxidizer enables the use of flame-based detection in chromatographic separations, such as carbon dioxide based chromatography, which employ polar modifiers, such as methanol. Upon exiting a chromatographic column, the mobile phase containing the polar modifier is flowed through an oxidizer that contains a catalyst to oxidize at least a portion of the polar modifier to a species that does not interfere with the function of the flame-based detector. The oxidizer allows for flame-based detection, such as flame ionization detection, in applications in which a polar modifier with a reduced form of carbon is used.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.