Method of making carbon nanotubes doped with iron, nitrogen and sulphur
US10439229B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Mar 15, 2017 |
| Grant date | Oct 8, 2019 |
| Priority date | — |
| Expiry date | Mar 15, 2037 |
Classification
- Technology area (CPC H)Electricity
- CPC primaryH01M12/06
- WIPO fieldMaterials, metallurgy
- WIPO sectorChemistry
Abstract
A method of making carbon nanotubes doped with iron, nitrogen and sulfur for an oxygen reduction reaction catalyst includes the steps of mixing an iron containing oxidizing agent with a sulfur-containing dye to form a fibrous fluctuate of reactive templates and using these for in-situ polymerization of an azo compound to form polymer-dye nanotubes, adding an alkali to precipitate magnetite, and subjecting the nanotubes to pyrolysis, acid leaching, and heat treatment.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.