Hollow iron-manganese composite material prepared by etching template process and application thereof
US10493425B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Nov 7, 2017 |
| Grant date | Dec 3, 2019 |
| Priority date | — |
| Expiry date | Feb 24, 2038 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC02F2101/20
- WIPO fieldChemical engineering
- WIPO sectorChemistry
Abstract
A method for preparing a hollow hydroxyl iron-manganese composite by employing a cubic structure template comprises: (1) preparation of a template: adding a certain mass of potassium permanganate to diluted hydrochloric acid, and dissolving and mixing evenly the same by magnetic stirring at room temperature; then adding polyvinylpyrrolidone thereto, and continuing to dissolve the same thoroughly by magnetic stirring; and finally adding a certain mass of potassium ferrocyanide and de-solubilizing the same for 10-60 minutes at room temperature, then transferring the above mixed solution into a sample bottle, and performing an isothermal reaction at 50-90° C. for 18-24 hours to obtain a blue-black deposit, namely a target iron-manganese composite template; and (2) preparation of a hollow iron-manganese composite: evenly dispersing the blue-black iron-manganese composite template obtained in the step (1) to a small amount of anhydrous ethanol, then adding a certain concentration of sodium hydroxide solution thereto, placing the same on a rotary shaker to react at room temperature for 6-12 hours, and then removing a supernatant liquid, so that a black substance remaining at a bottom of …
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.