Patent · US Active

Backfunctionalized imidazolinium salts and NHC carbene-metal complexes

US10538494B2 · kind B2 · utility

2Cited by
5References
7Claims
0Family size

Inventors

Key dates

Filing dateAug 14, 2018
Grant dateJan 21, 2020
Priority date
Expiry dateAug 14, 2038

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07F15/0046
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

Backfunctionalized imidazolinium salts and methods of synthesizing the same and NHC carbene-metal complexes therefrom. For backfunctionalized imidazolinium salts of the formula: Wherein R1 is selected from the group consisting of an ester group, an amide group, and an aromatic group; R2 is selected from the group consisting of hydrogen, an ester group, an amide group, and an aromatic group; R3 and R4 are each selected from the group consisting of a C1-C20 alkyl group, C1-C20 partially fluorinated alkyl group, an aryl group, an aryl group with para CF3 functionality, an aryl group having C1-C20 partially fluorinated alkyl groups or partially fluorinated alkoxy groups, and a C1-C20 partially fluorinated aliphatic group, and a C1-C20 aryl group; and X is an anion. The method comprises cyclization of a halogenated acrylate with a formamidine with Hünig's base in a solvent.

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