Method for preparing a NA3V2(PO4)2F3 particulate material
US11040881B2 · kind B2 · utility
Assignees
Inventors
Key dates
| Filing date | Oct 13, 2016 |
| Grant date | Jun 22, 2021 |
| Priority date | — |
| Expiry date | Nov 5, 2036 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY02E60/10
- WIPO fieldElectrical machinery, apparatus, energy
- WIPO sectorElectrical engineering
Abstract
A method for preparing a Na3V2(PO4)2F3 material, including at least the steps: a) reducing the vanadium oxide, V2O5, under a reducing atmosphere in the absence of elementary carbon and in the presence of at least one phosphate anion precursor in order to form vanadium phosphate, VPO4; and b) exposing, under an inert atmosphere, a mixture of the VPO4 material obtained in step a) with an effective amount of sodium fluoride, NaF, and at least one hydrocarbon- and oxygen-containing compound which is a source of elementary carbon, to temperature conditions that are favourable for calcining said mixture so as to form said Na3V2(PO4)2F3 compound. Also, a related electrode material, an electrode and a secondary sodium battery using the presented material.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.