Process for making solid methylglycine diacetate (MGDA) alkali metal salt, and solid particles
US11208375B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Feb 20, 2018 |
| Grant date | Dec 28, 2021 |
| Priority date | — |
| Expiry date | May 1, 2038 |
Classification
- Technology area (CPC B)Performing Operations; Transporting
- CPC primaryB01D2009/0086
- WIPO fieldChemical engineering
- WIPO sectorChemistry
Abstract
Process for making solid methylglycine diacetate (MGDA) alkali metal salt (a), said process comprising the steps of (A) providing a 35 to 60% by weight aqueous solution of said MGDA salt having a temperature in the range of from 50 to 90° C., (B) adding 0.01 to 2% by weight of a particulate solid with a pore volume in the range of from 0.25 to 0.75 cm3/g, determined by nitrogen adsorption in accordance with 66134:1998-02 (b), the percentage referring to the content of (a), (C) crystallizing (a), (D) removing said crystalline (a) from the mother liquor.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.