Patent · US Active

Method for manufacturing ammonia synthesis catalyst, and method for manufacturing ammonia

US11235310B2 · kind B2 · utility

17Cited by
1References
13Claims
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Key dates

Filing dateAug 8, 2017
Grant dateFeb 1, 2022
Priority date
Expiry dateNov 8, 2037

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY02P20/52
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

Provided is a method for manufacturing a catalyst with which it is possible to obtain a supported metal ammonia synthesis catalyst, in which there are restrictions in terms of producing method and producing facility, and particularly large restrictions for industrial-scale producing, in a more simple manner and so that the obtained catalyst has a high activity. This method for manufacturing an ammonia synthesis catalyst includes: a first step for preparing 12CaO.7Al2O3 having a specific surface area of 5 m2/g or above; a second step for supporting a ruthenium compound on the 12CaO.7Al2O3; and a third step for performing a reduction process on the 12CaO.7Al2O3 supporting the ruthenium compound, obtained in the second step. This invention is characterized in that the reduction process is performed until the average particle diameter of the ruthenium after the reduction process has increased by at least 15% in relation to the average particle diameter of the ruthenium before the reduction process.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.