Patent · US Active

Low-energy consumption method for dehydrating ethanol into ethylene

US11358911B2 · kind B2 · utility

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1References
24Claims
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Key dates

Filing dateNov 27, 2019
Grant dateJun 14, 2022
Priority date
Expiry dateNov 27, 2039

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07C2529/40
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

A process for dehydrating an ethanol feedstock to give ethylene, includes:a) a vaporization stage;b) a heating stage;c) a dehydration stage in a multitubular reactor comprising tubes having a length of between 2 and 4 m, said tubes comprising a, preferably zeolitic, dehydration catalyst, the feedstock having an inlet temperature of greater than 400° C. and less than 550° C. and an inlet pressure of between 0.8 and 1.8 MPa, the heat transfer fluid having an inlet temperature of greater than 430° C. and less than 550° C. and a mass flow rate such that the ratio of the mass flow rates of the heat transfer fluid relative to the feedstock is greater than or equal to 10;d) separation into an effluent comprising ethylene and an aqueous effluent;e) purification of the aqueous effluent and separation of a stream of purified water and a stream of unconverted ethanol.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.