Process for the separation of diols
US11384039B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | May 19, 2017 |
| Grant date | Jul 12, 2022 |
| Priority date | — |
| Expiry date | Nov 7, 2039 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07C29/80
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
The invention provides a process for the separation of a first C3 to C7 diol from a first mixture of C3 to C7 diols. The first mixture is provided to a first distillation column. An extractant is fed to the first distillation column above the first mixture. A stream comprising the first diol and the extractant is removed as a bottoms stream from the first distillation column and subjected to distillation in a second distillation column. A high purity first diol stream is removed from the top section of the second distillation column, while a used extractant stream is removed from the bottom section. The extractant is a C3 to C6 sugar alcohol or mixture thereof. The first diol is a close-boiler to and/or forms an azeotrope with one or more of the other C3 to C7 diols present in the first mixture.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.