Method for producing lithium titanium phosphate
US11404720B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Jan 27, 2020 |
| Grant date | Aug 2, 2022 |
| Priority date | — |
| Expiry date | Jan 27, 2040 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY02E60/10
- WIPO fieldElectrical machinery, apparatus, energy
- WIPO sectorElectrical engineering
Abstract
An X-ray diffractometrically single-phase lithium titanium phosphate can be obtained by an industrially advantageous method. Provided is a method for producing the lithium titanium phosphate having a NASICON structure represented by the following general formula (1): Li1+xMx(Ti1−yAy)2−x(PO4)3 (1), and provided is a method comprising a first step of preparing a raw material mixed slurry (1) comprising, at least, titanium dioxide, phosphoric acid and a surfactant, a second step of heat treating the raw material mixed slurry (1) to obtain a raw material heat-treated slurry (2), a third step of mixing the raw material heat-treated slurry (2) with a lithium source to obtain a lithium-containing raw material heat-treated slurry (3), a fourth step of subjecting the lithium-containing raw material heat-treated slurry (3) to a spray drying treatment to obtain a reaction precursor containing, at least, Ti, P and Li, and a fifth step of firing the reaction precursor.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.