Titanium sub-oxide/ruthenium oxide composite electrode and preparation method and application thereof
US11519088B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Mar 11, 2020 |
| Grant date | Dec 6, 2022 |
| Priority date | — |
| Expiry date | May 27, 2041 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC02F2305/08
- WIPO fieldSurface technology, coating
- WIPO sectorChemistry
Abstract
A titanium sub-oxide/ruthenium oxide composite electrode and a preparation method and application thereof. Titanium-based titanium sub-oxide nanotubes is taken as a bottom layer, and titanium sub-oxide doped ruthenium oxide is taken as a surface composite active layer. A titanium substrate is anodized in a fluorine-containing ionic electrolyte, taken out, subjected to heating and roasting, cooled and then subjected to cathodic electrochemical reduction in polarizing liquid, so that a titanium-based titanium sub-oxide nanotube electrode is obtained; and then the titanium-based titanium sub-oxide nanotube electrode is taken as a cathode to be electrodeposited in a ruthenium trichloride electrolyte doped with titanium sub-oxide powder, taken out and then subjected to heating and roasting, so that the titanium sub-oxide/ruthenium oxide composite electrode is obtained.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.