Battery-level Ni—Co—Mn mixed solution and preparation method for battery-level Mn solution
US11695170B2 · kind B2 · utility
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Key dates
| Filing date | Dec 31, 2019 |
| Grant date | Jul 4, 2023 |
| Priority date | — |
| Expiry date | Dec 31, 2039 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY02W30/84
- WIPO fieldMaterials, metallurgy
- WIPO sectorChemistry
Abstract
Provided are a battery-level Ni—Co—Mn mixed solution and a preparation method for a battery-level Mn solution, the steps thereof comprising: acid dissolution (S1), alkalization to remove impurities (S2), synchronous precipitation of calcium, magnesium, and lithium (S3), deep ageing to remove impurities (S4), synergistic extraction (S5), and refining extraction (S6). The steps of deep ageing to remove impurities (S4) and synergistic extraction (S5) comprise: performing deep ageing on a filtrate obtained from the step of synchronous precipitation of calcium, magnesium, and lithium (S3), and after performing filtration to remove impurities, obtaining an aged filtrate; using P204 to extract the aged filtrate and obtain a loaded organic phase, and subjecting the loaded organic phase to staged back-extraction to obtain the battery-level Ni—Co—Mn mixed solution and a Mn-containing solution. By means of the cooperation between the multiple process steps of synchronous precipitation of calcium, magnesium, and lithium (S3), deep ageing to remove impurities (S4), and synergistic extraction (S5), the impurity content of the obtained battery-level Ni—Co—Mn mixed solution is significantly lowere…
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.