Fluorine-containing polycaprolactone film and preparation method therefor
US11807728B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Nov 29, 2020 |
| Grant date | Nov 7, 2023 |
| Priority date | — |
| Expiry date | Jul 23, 2042 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC08J2367/04
- WIPO fieldMacromolecular chemistry, polymers
- WIPO sectorChemistry
Abstract
A method of preparing a fluorinated polycaprolactone membrane includes the following steps: (1) reacting a polycaprolactone with an aminoalcohol compound to prepare a hydroxyl-terminated polycaprolactone; (2) reacting the hydroxyl-terminated polycaprolactone with an anhydride to prepare a carboxyl-terminated polycaprolactone; (3) reacting an ethylene glycol bromoisobutyrate with a fluorinated acrylate to prepare a hydroxyl-terminated fluoro-acrylate polymer; (4) reacting the carboxyl-terminated polycaprolactone with the hydroxyl-terminated fluoro-acrylate polymer to prepare a fluorinated polycaprolactone; (5) at room temperature, dissolving the fluorinated polycaprolactone in an organic solvent to prepare a solution; then naturally drying the solution at room temperature to prepare the fluorinated polycaprolactone membrane.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.