Patent · US Active

Method for measuring terephthalic acid content and solvent for use in measurement

US11867647B2 · kind B2 · utility

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10Claims
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Key dates

Filing dateMay 10, 2019
Grant dateJan 9, 2024
Priority date
Expiry dateFeb 25, 2041

Classification

  • Technology area (CPC G)Physics
  • CPC primaryG01N24/08
  • WIPO fieldMeasurement
  • WIPO sectorInstruments

Abstract

In a first step, a sample liquid is fabricated by mixing a sample formed of a polyester or decomposition products of a polyester into a solvent. The solvent used here contains chloroform and 2,2,2-trifluoroethanol and has an organic base added thereto. The organic base is at least one of a primary amine, a secondary amine, a tertiary amine and a heterocyclic amine. In a second step, the amount of terephthalic acid in the sample liquid is measured through a nuclear magnetic resonance spectroscopy aiming at hydrogen atoms

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.