Removal of Al-salts, HCl, NaCl and organic by-product from strong alkaline DIOPAT suspension by means of alkaline stable nanofiltration followed by separation of salts and byproducts after neutralization of DIOPAT solution by means of ultrafiltration
US11904279B2 · kind B2 · utility
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19Claims
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Key dates
| Filing date | Oct 30, 2019 |
| Grant date | Feb 20, 2024 |
| Priority date | — |
| Expiry date | Oct 1, 2040 |
Classification
- Technology area (CPC B)Performing Operations; Transporting
- CPC primaryB01D2315/16
- WIPO fieldChemical engineering
- WIPO sectorChemistry
Abstract
The present invention provides an improved process for isolating 2,4-bis-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazine (DIOPAT) from an aqueous alkaline mixture M having a pH of 10 or more and comprising the 2,4-bis-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazine, 2,4-dihydroxybenzophenone, and aluminum salts, wherein the process comprises a nanofiltration step, a precipitation step, and a further filtration step.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.