Method of preparing diene-based rubber polymer and method of preparing graft polymer including the diene-based rubber polymer
US12103998B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Aug 24, 2020 |
| Grant date | Oct 1, 2024 |
| Priority date | — |
| Expiry date | Feb 24, 2042 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY02T10/86
- WIPO fieldMacromolecular chemistry, polymers
- WIPO sectorChemistry
Abstract
Provided is a method of preparing a diene-based rubber polymer, which includes: adding each of a diene-based monomer, a molecular-weight regulator, an initiator, and an emulsifier to a reactor a first time and carrying out polymerization; adding a molecular-weight regulator to the reactor a second time when a polymerization conversion rate of 48 to 72% is reached and carrying out polymerization; adding a diene-based monomer to the reactor a second time when a polymerization conversion rate of 63 to 77% is reached and carrying out polymerization; adding each of an initiator and an emulsifier to the reactor a second time when a polymerization conversion rate of 68 to 81% is reached and carrying out polymerization; and adding each of an initiator and an emulsifier to the reactor a third time when a polymerization conversion rate of 85 to 91% is reached and carrying out polymerization.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.