Patent · US Active

Preparation method for bio-based nucleating agent for poly(ethylene furandicarboxylate) and application thereof

US12252601B1 · kind B1 · utility

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Key dates

Filing dateJul 19, 2024
Grant dateMar 18, 2025
Priority date
Expiry dateJul 19, 2044

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC08K5/098
  • WIPO fieldMacromolecular chemistry, polymers
  • WIPO sectorChemistry

Abstract

Aiming at the problem of slow crystallization rate of poly(ethylene furandicarboxylate) (PEF), a preparation method for a bio-based nucleating agent for PEF and an application thereof are disclosed. In a technical solution, glycine having a bio-based source is subjected to an amidation reaction with furoic acid under the catalysis of p-toluenesulfonic acid, followed by an acid-base neutralization reaction with sodium hydroxide to obtain a bio-based nucleating agent for PEF. The bio-based nucleating agent prepared by the present disclosure can significantly accelerate a crystallization rate of PEF. Most importantly, the bio-based nucleating agent has no effect on the bio-based properties of PEF.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.