Removal of Al-salts, HCl, NaCl and organic by-product from DIOPAT suspension by means of ceramic membranes in strong acidic conditions at high temperature
US12304891B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Jul 18, 2019 |
| Grant date | May 20, 2025 |
| Priority date | — |
| Expiry date | Jul 13, 2042 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC02F1/66
- WIPO fieldChemical engineering
- WIPO sectorChemistry
Abstract
The present invention provides an improved process for isolating 2,4-bis-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazine (DIOPAT) from an aqueous alkaline mixture M comprising the DIOPAT, 2,4-dihydroxybenzophenone, and aluminum salts, wherein the process comprises the steps of precipitating the DIOPAT by acidifying the mixture M to a pH<1; heating the acidified mixture M to a temperature in the range of from 80° C. to 95° C.; and separating of the precipitated DIOPAT from the dissolved 2,4-dihydroxybenzophenone and the dissolved aluminum salts with a ceramic membrane by means of diafiltration.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.