Patent · US Active

Removal of Al-salts, HCl, NaCl and organic by-product from DIOPAT suspension by means of ceramic membranes in strong acidic conditions at high temperature

US12304891B2 · kind B2 · utility

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17Claims
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Key dates

Filing dateJul 18, 2019
Grant dateMay 20, 2025
Priority date
Expiry dateJul 13, 2042

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC02F1/66
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

The present invention provides an improved process for isolating 2,4-bis-(2,4-dihydroxyphenyl)-6-(4-methoxyphenyl)-1,3,5-triazine (DIOPAT) from an aqueous alkaline mixture M comprising the DIOPAT, 2,4-dihydroxybenzophenone, and aluminum salts, wherein the process comprises the steps of precipitating the DIOPAT by acidifying the mixture M to a pH<1; heating the acidified mixture M to a temperature in the range of from 80° C. to 95° C.; and separating of the precipitated DIOPAT from the dissolved 2,4-dihydroxybenzophenone and the dissolved aluminum salts with a ceramic membrane by means of diafiltration.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.