Methods for preparing supported catalysts using waste lithium batteries and attapulgite
US12322772B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Nov 25, 2024 |
| Grant date | Jun 3, 2025 |
| Priority date | — |
| Expiry date | Nov 25, 2044 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY02W30/84
- WIPO fieldChemical engineering
- WIPO sectorChemistry
Abstract
A method for preparing a supported catalyst, including mixing waste lithium battery cathode material and biomass uniformly to obtain a mixture, then putting the mixture into a tube furnace for nitrogen purging, and then heating and calcining to obtain a solid sample after carbothermal reduction treatment; hydrothermally stirring the solid sample, followed by filtration to recover a residue, and drying the residue to obtain a mixed sample of Co3O4, TiO2, and biochar, labeled as TCO; ultrasonically dispersing the attapulgite in an acid solution, stirring in a water bath at 80° C. to obtain a product, washing the product until neutral, filtering, and then drying to obtain an acidified attapulgite (H-ATP); and weighing the TCO, ultrasonically dispersing the TCO in a mixed solution of deionized water and N, N dimethylformamide (DMF), adding the H-ATP into the mixed solution, and performing a microwave hydrothermal reaction, obtaining a sample after centrifuging, washing, and drying, and then performing muffle calcination on the sample to obtain the supported catalyst Co3(Ti)O4/H-ATP.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.