Patent · US Active

Nickel foam-supported defective tricobalt tetroxide nanomaterial, low temperature resistant supercapacitor and preparation method thereof

US12347618B2 · kind B2 · utility

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6Claims
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Key dates

Filing dateJan 14, 2021
Grant dateJul 1, 2025
Priority date
Expiry dateFeb 22, 2042

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY02E60/13
  • WIPO fieldElectrical machinery, apparatus, energy
  • WIPO sectorElectrical engineering

Abstract

The present invention relates to the field of electrode material of a low temperature resistant supercapacitor, and in particular to a nickel foam-supported defective tricobalt tetroxide nanomaterial, a low temperature resistant supercapacitor and a preparation method thereof. The method includes the following steps: dissolving cobalt acetate in an ethylene glycol solution and stirring uniformly to obtain a pink transparent solution; adding hexadecyl trimethyl ammonium bromide to the pink transparent solution, and stirring until the hexadecyl trimethyl ammonium bromide dissolves to obtain a mixed solution; putting the mixed solution into a teflon-lined reactor, adding pretreated nickel foam for hydrothermal reaction, taking out the nickel foam after the reaction is completed, and ultrasonic cleaning the nickel foam repeatedly before drying; and heat-treating the nickel foam obtained after drying. The defective tricobalt tetroxide (D-Co3O4) grown on the nickel foam prepared by the present invention still has a high specific capacity at a low temperature, and the assembled supercapacitor can withstand low temperature, and thus has great application prospects.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.