Patent · US Active

LC-MS methods for antibody isotyping and quantification

US12411141B2 · kind B2 · utility

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50Claims
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Assignee

Inventors

Key dates

Filing dateSep 16, 2020
Grant dateSep 9, 2025
Priority date
Expiry dateDec 29, 2041

Classification

  • Technology area (CPC G)Physics
  • CPC primaryG01N2800/52
  • WIPO fieldMeasurement
  • WIPO sectorInstruments

Abstract

The present invention provides methods and systems for isotyping and quantification of antibodies based on immunocapture and/or Liquid Chromatography-Mass Spectrometry (LC-MS) analysis. These antibodies are induced by the administration of pharmaceutical products. The immunocapture method comprises contacting samples with a solid support, wherein the pharmaceutical product has been cross-linked directly to the solid support. The MS analysis includes conducting peptide mapping, selecting unique peptides and fragment ions to generate MRM (multiple reaction monitoring) transitions, optimizing collision energy, and determining a LLOQ (lower limit of quantification).

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.