Process for the production of pure tetrazole-1-acetic acid
US3932441A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Sep 27, 1974 |
| Grant date | Jan 13, 1976 |
| Priority date | — |
| Expiry date | Sep 27, 1994 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07D257/04
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
Process for producing tetrazole-1-acetic acid of maximum purity includes the steps of providing a crude reaction product containing an alkyl ester of tetrazole-1-acetic acid having from 1 to 4 carbon atoms in the alkyl group, effecting molecular distillation of this reaction product at a temperature below 130.degree.C. under a vacuum of 10.sup.-.sup.1 torr to obtain a distillant containing the alkyl ester and then gently hydrolyzing the resultant distillate to obtain the desired acid product.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.