Process for recovering resorcinol and hydroquinone in mixture
US3969420A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Jul 2, 1973 |
| Grant date | Jul 13, 1976 |
| Priority date | — |
| Expiry date | Jul 2, 1993 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07C37/84
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
Resorcinol and hydroquinone are recovered in mixture at a high purity from a solution containing resorcinol and hydroquinone, especially, a solution resulting from cleavage of oxidation products of isopropylbenzene and successive distillation of the cleavage product thereby to remove lower and higher boiling components therefrom, by adding 0.5 to 20 parts by weight of at least one solvent selected from aromatic hydrocarbons, aromatic hydrocarbons having lower alkyl substituent groups, and aliphatic hydrocarbons having 7 to 10 carbon atoms to one part by weight of said solution, if necessary, together with 1 to 30% by weight of at least one compound selected from ketones having 3 to 10 carbon atoms, alcohols having 1 to 5 carbon atoms and aliphatic esters having 3 to 5 carbon atoms, based on the weight of the organic solvent, dissolving the solution into the organic solvent by heating, separating a mixture of resorcinol and hydroquinone as a solid phase from the organic solvent layer after slow cooling, and recovering the solid phase as a product. The resorcinol and hydroquinone in the organic solvent layer are further recovered through extraction with water. When water is used toge…
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.