Patent · US Expired

Flotation process for removal of precipitates from electrochemical chromate reduction unit

US3989608A · kind A · utility

18Cited by
6References
8Claims
0Family size

Assignee

Inventors

Key dates

Filing dateDec 30, 1975
Grant dateNov 2, 1976
Priority date
Expiry dateDec 30, 1995

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC02F2103/023
  • WIPO fieldEnvironmental technology
  • WIPO sectorChemistry

Abstract

This invention is an improved form of a conventional electrochemical process for removing hexavalent chromium or other metal-ion contaminants from cooling-tower blowdown water. In the conventional process, the contaminant is reduced and precipitated at an iron anode, thus forming a mixed precipitate of iron and chromium hydroxides, while hydrogen being evolved copiously at a cathode is vented from the electrochemical cell. In the conventional process, subsequent separation of the fine precipitate has proved to be difficult and inefficient. In accordance with this invention, the electrochemical operation is conducted in a novel manner permitting a much more efficient and less expensive precipitate-recovery operation. That is, the electrochemical operation is conducted under an evolved-hydrogen partial pressure exceeding atmospheric pressure. As a result, most of the evolved hydrogen is entrained as bubbles in the blowdown in the cell. The resulting hydrogen-rich blowdown is introduced to a vented chamber, where the entrained hydrogen combines with the precipitate to form a froth which can be separated by conventional techniques. In addition to the hydrogen, two materials present in …

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.