Preparation of trichlorothiazole and intermediate
US4018784A · kind A · utility
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2References
7Claims
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Key dates
| Filing date | Dec 9, 1975 |
| Grant date | Apr 19, 1977 |
| Priority date | — |
| Expiry date | Dec 9, 1995 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07D277/32
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
Trichlorothiazole of the formula ##STR1## IS PREPARED BY REACTING 1,2,2,2-TETRACHLOROETHYL-ISOCYANIDEDICHLORIDE OF THE FORMULA ##STR2## WITH 1 TO 1.2 TIMES THE STOICHIOMETRIC AMOUNT OF SULFUR AT A TEMPERATURE OF ABOUT 150.degree. TO 250.degree. C, preferably about 170.degree. to 230.degree. C.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.