Process for preparing organosiloxanes
US4032557A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Apr 26, 1976 |
| Grant date | Jun 28, 1977 |
| Priority date | — |
| Expiry date | Apr 26, 1996 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07F7/21
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
An improved process for preparing organosiloxanes and alkyl halides by passing organohalosilanes and alkanols having 1 and/or 2 carbon atoms through at least one layer of packing material which is maintained at a temperature of from 60.degree. to 150.degree. C, the improvement which comprises (1) recycling from 1 to 6 liters of an aqueous phase separated from the organosiloxanes emerging from the layer or layers of packing material for each mol of organohalosilane introduced into the layer or layers of packing material and (2) reacting the organosiloxane separated from the aqueous phase with from 2 to 10 percent by weight based on the weight of the organosiloxane with the same organohalosilane which is passed through the layer or layers of packing material.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.