Method of removing water from liquid olefin in the polymerization of olefins
US4068053A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Sep 30, 1976 |
| Grant date | Jan 10, 1978 |
| Priority date | — |
| Expiry date | Sep 30, 1996 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC08F110/06
- WIPO fieldMacromolecular chemistry, polymers
- WIPO sectorChemistry
Abstract
Removing water and light ends from recycle liquid olefin monomer and fresh liquid olefin monomer feed before catalytic polymerization thereof in said liquid state with a water sensitive catalyst, by flowing them through a mass transfer plate tower with a reboiler which vaporizes them upwardly through openings in the plates of said tower and in the form of bubbles through layers of liquid monomer reflux maintained on said plates by weirs and downcomers by means of which said reflux is flowed from each plate downwardly to the plate below it and, as a layer, along the top of the plate and thence downwardly to the next lower plate, condensing in a reflux condenser the vapor from the top of said tower, removing from said condenser as a vapor said light ends, removing water from said condenser as a heavy condensed liquid fraction and refluxing back to the top of said tower as a lighter liquid fraction, condensed liquid monomer. Preferably the tower is a valve tray tower and the plates are valve trays.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.