Patent · US Expired

Silica polymorph and process for preparing same

US4073865A · kind A · utility

113Cited by
1References
6Claims
0Family size

Assignee

Inventors

Key dates

Filing dateSep 27, 1976
Grant dateFeb 14, 1978
Priority date
Expiry dateSep 27, 1996

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10S423/22
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

Large crystals of a silica polymorph having a characteristic X-ray diffraction pattern, a specific gravity of 1.70 .+-. 0.05 g/cc. and a mean refractive index of 1.39 .+-. 0.01 after calcination in air at 600.degree. C., are prepared by a hydrothermal process in which fluoride anions are included in the reaction mixture. The crystals, which can be as large as 200 microns, exhibit a substantial absence of infrared adsorption in the hydroxyl-stretching region and also exhibit an exceptional degree of hydrophobicity.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.