Patent · US Expired

Process for preparing tetrahydrofuran

US4093633A · kind A · utility

14Cited by
3References
10Claims
0Family size

Assignee

Inventors

Key dates

Filing dateJan 28, 1977
Grant dateJun 6, 1978
Priority date
Expiry dateJan 28, 1997

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07D307/08
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

In the process for preparing tetrahydrofuran by the dehydrocyclization of 1,4-butanediol in the presence of a non-volatile acid catalyst, wherein vapor mixture of water and tetrahydrofuran is continuously taken out from the reaction zone and subjected to the azeotropic distillation in three distillation columns operated under specified conditions thereby obtaining tetrahydrofuran of high quality in a high yield.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.