Electrochemical coupling of perfluoroalkyl iodides
US4097344A · kind A · utility
12Cited by
2References
10Claims
0Family size
Assignee
Inventor
Key dates
| Filing date | Jun 29, 1976 |
| Grant date | Jun 27, 1978 |
| Priority date | — |
| Expiry date | Jun 29, 1996 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC25B3/29
- WIPO fieldSurface technology, coating
- WIPO sectorChemistry
Abstract
A process of anodically coupling compounds of the formula R.sup.1.sub.f R.sup.2.sub.f CFI where R.sup.1.sub.f and R.sup.2.sub.f are each independently fluorine or a perfluoroalkyl radical containing from 4 to 40 carbon atoms in a liquid carboxylic acid in the presence of a small amount of carboxylate ion. The process generally is carried out at from 25.degree. to 150.degree. C. Generally the concentration of R.sup.1.sub.f R.sup.2.sub.f CFI is from 5 to 40 weight percent of the reaction mixture.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.