Patent · US Expired

Method to generate correlative data from various products of thermal degradation of biological specimens

US4122343A · kind A · utility

24Cited by
0References
10Claims
0Family size

Assignee

Inventors

Key dates

Filing dateMar 14, 1977
Grant dateOct 24, 1978
Priority date
Expiry dateMar 14, 1997

Classification

  • Technology area (CPC G)Physics
  • CPC primaryG01N31/12
  • WIPO fieldMeasurement
  • WIPO sectorInstruments

Abstract

In a method generating correlative data from various products of thermal degradation of biological specimens and comprising sequential steps for each specimen of degrading such specimen by heating such specimen so as to cause various products of thermal degradation of such specimen to be evolved, ionizing the products of thermal degradation of such specimen by a technique causing negligible fragmentation, detecting ion currents for such specimen, and recording such detected ion currents, an improvement is attained wherein each specimen is heated in an identical non-isothermal time-dependent heating sequence, wherein a three-dimensional array comprising a large and sufficient number of ion currents, which correspond to substantially all detectible ratios of mass-to-charge within a range at a large and sufficient number of successive instants during the respective heating sequences, are detected and recorded for each specimen, and representative data from the three-dimensional array thus recorded for each one of such specimens are correlated to representative data from the three-dimensional array thus recorded for each other of the specimens. Therein, one dimension of each array repr…

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