Patent · US Expired

Process for regenerating water-containing methanol

US4144314A · kind A · utility

20Cited by
3References
15Claims
0Family size

Assignee

Inventors

Key dates

Filing dateSep 26, 1977
Grant dateMar 13, 1979
Priority date
Expiry dateSep 26, 1997

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC10K1/165
  • WIPO fieldBasic materials chemistry
  • WIPO sectorChemistry

Abstract

An improvement in a process for regenerating a water-containing, highly volatile organic solvent which has been used to scrub acid constituents from gases having a low content of water and of volatile compounds of the 8th group of the Periodic System is disclosed. According to the process, solvent which contains absorbed acid constituents is regenerated in a regeneration zone by heating the same to drive off acid constituents and deacidified solvent is recycled in the scrubbing process. According to the invention the solvent is contacted during the regeneration with a complexing agent soluble in the solvent in an amount of 0.005 to 1 gram complexing agent per liter of solvent. A branch stream is removed from the regeneration zone which branch stream contains volatile solvent, water and metal salts dissolved in the water. The branch stream is subjected to distillation to remove overhead the volatile solvent which is returned to the regeneration zone and to leave behind an aqueous solution of the metal salt. A compensating amount of water is added to the solvent cycle.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.