Patent · US Expired

Synthesizing low sodium crystalline aluminosilicate zeolites with primary amines

US4151189A · kind A · utility

56Cited by
2References
14Claims
0Family size

Assignee

Inventors

Key dates

Filing dateApr 10, 1978
Grant dateApr 24, 1979
Priority date
Expiry dateApr 10, 1998

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10S423/22
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

A method is disclosed for synthesizing a crystalline aluminosilicate zeolite containing an organic nitrogen cation in the presence of a primary monoalkylamine having 2 to 9 carbon atoms in the alkyl portion. The method produces a zeolite having a very low percentage, i.e. less than about 0.14 weight percent, generally less than about 0.1 weight percent of alkali metal, e.g. sodium, in the as-synthesized form. The product can be used directly as a catalyst without intermediate precalcination and cation exchange. This is not possible with zeolites such as those of the ZSM-5 type synthesized by the methods of the art.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.