Patent · US Expired

Synthesis of steroids

US4174345A · kind A · utility

13Cited by
0References
12Claims
0Family size

Inventor

Key dates

Filing dateAug 1, 1978
Grant dateNov 13, 1979
Priority date
Expiry dateAug 1, 1998

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07J9/005
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

In the synthesis of sterols wherein methoxyethoxymethyl groups in an ether linkage are attached to the nucleus of the sterol to protect the sterol nucleus during other steps of the synthesis and the sterols are thereafter treated to remove the methoxyethoxymethyl groups and set free the hydroxyl groups, the improvement in which the sterols being treated with zinc bromide are held in a methylene chloride solution containing a small amount of an aliphatic alcohol having from 1 to 6 carbon atoms.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.