Patent · US Expired

Novel bicyclic scents

US4224253A · kind A · utility

2Cited by
6References
3Claims
0Family size

Assignee

Inventors

Key dates

Filing dateAug 28, 1978
Grant dateSep 23, 1980
Priority date
Expiry dateAug 28, 1998

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07C2602/42
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

Novel 2-methylene-3-methyl-3-(1',3'-pentadien-1'-yl)-bicyclo-[2,2,1]-heptanes substituted in the 4'-position by methyl, alkoxycarbonyl, formyl, hydroxymethyl or cyano are obtained by reacting the novel aldehyde 2-methylene-3-methyl-3-formyl-bicyclo-[2,2,1]-heptane with 3-methyl-, 3-alkoxycarbonyl- or acetalized 3-formyl-2-butene-1-triarylphosphorylidene under the conditions of a Wittig reaction, with or without hydrolytic cleavage of the acetal group, or hydrolytic cleavage of the acetal group followed by reduction of the formyl group to the hydroxymethyl group, or hydrolytic cleavage of the acetal group, reaction of the aldehyde with a hydroxylammonium salt, and dehydration of the resulting oxime. The novel compounds are distinguished by interesting scent characteristics.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.