Patent · US Expired

Granulation of sodium metasilicate

US4253849A · kind A · utility

4Cited by
5References
20Claims
0Family size

Assignee

Inventors

Key dates

Filing dateSep 26, 1978
Grant dateMar 3, 1981
Priority date
Expiry dateSep 26, 1998

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC01B33/325
  • WIPO fieldMaterials, metallurgy
  • WIPO sectorChemistry

Abstract

Sodium metasilicate is granulated by (i) establishing, in a first zone, a cloud of anhydrous sodium metasilicate powder; (ii) injecting into said cloud (i), and intimately contacting therewith, an atomized liquid phase which comprises a liquid formulation of a sodium silicate; (iii) said intimate contacting (ii) being conducted in an atmosphere of a drying gas, whereby crystallization of the anhydrous metasilicate and agglomeration of the thus coated particulates are effected, (iv) next subjecting the effluent cohered granules of said first zone to a state of agitation in a second discrete zone, in an atmosphere of a heating gas and whereby the agitated granules are at least partially converted to the sodium metasilicate pentahydrate; (v) and thence recovering from said second discrete zone a granular sodium metasilicate comprising from about 2 to 6% by weight water, and useful in the manufacture of a variety of detergent compositions.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.