Preparation of bis-2-pyridyl-disulfides
US4256892A · kind A · utility
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8Claims
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Key dates
| Filing date | Nov 8, 1979 |
| Grant date | Mar 17, 1981 |
| Priority date | — |
| Expiry date | Nov 8, 1999 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07D213/71
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
In a process for the preparation of bis-2-pyridyl-disulfide or bis-(2-pyridyl-1-oxide)-disulfide optionally substituted on the pyridyl ring with at least one substituent selected from the group consisting of halogen and alkyl and alkoxy of 1 to 4 carbon atoms by oxidation of the corresponding 2-mercapto-pyridine or its N-oxide, the improvement comprising effecting the oxidation in an aqueous acid media containing an alkali metal or alkaline earth metal chlorite.
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