Patent · US Expired

Antitumor glycosides, their preparation and use

US4276289A · kind A · utility

0Cited by
4References
5Claims
0Family size

Assignee

Inventors

Key dates

Filing dateMar 17, 1980
Grant dateJun 30, 1981
Priority date
Expiry dateMar 17, 2000

Classification

  • Technology area (CPC A)Human Necessities
  • CPC primaryA61P35/00
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

Anthracycline glycosides of the formula I ##STR1## wherein R is hydrogen or hydroxyl and the hydrochlorides thereof, and which are useful in treating certain mammalian tumors, are prepared by condensing daunomycinone with the novel sugar, 4-O-methyl-2,3,6-trideoxy-3trifluoroacetamidoribohexopyranosyl chloride in an inert organic solvent and in the presence of a soluble silver salt and a dehydrating agent to form 3', 4' -diepi-4'-O-methyl-N-trifluoroacetyl daunorubicin, and removing the N-trifluoroacetyl group therefrom. This gives the compound wherein R is hydrogen. The former is converted to the corresponding hydroxyl compound by conventional means.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.