Process for preparing the compound 5-t-butyl-2-methylamino-1,3,4-triadiazole
US4283543A · kind A · utility
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Key dates
| Filing date | Oct 19, 1979 |
| Grant date | Aug 11, 1981 |
| Priority date | — |
| Expiry date | Oct 19, 1999 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07D285/135
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
A process for preparing the compound 5-t-butyl-2-methylamino-1,3,4-thiadiazole, ##STR1## in high yield by the reaction of 4-methyl-3-thiosemicarbazide with pivalic acid in a solution containing both polyphosphoric acid and concentrated sulfuric acid, followed by neutralizing the reaction mixture with a neutralizing mixture comprising an organic solvent and an alkaline substance dissolved in water and separating 5-t-butyl-2-methylamino-1,3,4-thiadiazole from the organic phase.
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