Patent · US Expired

Zone purification of cylindrical ingots

US4285760A · kind A · utility

1Cited by
4References
3Claims
0Family size

Assignee

Inventor

Key dates

Filing dateOct 25, 1979
Grant dateAug 25, 1981
Priority date
Expiry dateOct 25, 1999

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10T117/108
  • WIPO fieldSurface technology, coating
  • WIPO sectorChemistry

Abstract

Cylindrical ingots of materials that expand on melting or freezing are purified or zone refined by a process which includes providing a tubular container having both a cylindrical cavity and a slot along its entire length. In zone refining, as is well-known, a heater of a predetermined elevated temperature traverses from one end of a normally solid charge to another at least once to thereby sweep impurities to one end of the charge. During the zone refining process, material which expands on phase change (e.g., solid to liquid) flows into the slot. As a consequence, fractures and other damage to the container and/or zone-refined material are minimized. The substantially round cross section is retained following removal of the excess material from the zone refined ingot after solidification.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.