Patent · US Expired

Lignin-containing resin adhesive

US4303562A · kind A · utility

20Cited by
9References
10Claims
0Family size

Assignee

Inventors

Key dates

Filing dateJul 24, 1980
Grant dateDec 1, 1981
Priority date
Expiry dateJul 24, 2000

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC09J197/005
  • WIPO fieldMacromolecular chemistry, polymers
  • WIPO sectorChemistry

Abstract

Novel lignin-phenol-formaldehyde resins, suitable for use as wood bonding adhesives, are provided by a two-step method which comprises reacting formaldehyde and phenol in the presence of an alkaline catalyst for a period sufficient to produce a partially condensed phenol-formaldehyde resin, thereafter reacting said precondensed resin with sodium hydroxide, formaldehyde and a lignin concentrate having at least 40% solids and comprising lignin dissolved in (a) phenol and water; or (b) phenol, water and sodium hydroxide or ammonia, the lignin to phenol weight ratios in said solution being less than 70:30 and more than 40:60. The second stage of the method is conducted at reflux temperature initially after which reaction is conducted below reflux temperature to control the degree of condensation.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.