Process for the isolation of monochloroacetaldehyde
US4311563A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Mar 31, 1981 |
| Grant date | Jan 19, 1982 |
| Priority date | — |
| Expiry date | Mar 31, 2001 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07C45/82
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
The invention relates to a process for the isolation of chloroacetaldehyde which is obtained as a by-product during the synthesis of acetaldehyde from ethylene and air in an aqueous palladium/cupric chloride solution by the 2-stage process. The mixture to be worked-up to chloroacetaldehyde is taken from the acetaldehyde distillation column and transferred to a distillation and extraction system, where it is fractionally condensed. The chloroacetaldehyde-containing fraction is extracted with water and the aqueous extract is subjected to purification distillation.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.