Patent · US Expired

Process and device for the preparation of a product containing ammonium orthophosphate, and product obtained by this process

US4313918A · kind A · utility

3Cited by
6References
8Claims
0Family size

Assignee

Inventors

Key dates

Filing dateMay 29, 1979
Grant dateFeb 2, 1982
Priority date
Expiry dateMay 29, 1999

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10S261/75
  • WIPO fieldMaterials, metallurgy
  • WIPO sectorChemistry

Abstract

Ammonium orthophosphate products are prepared by reacting ammonia and phosphoric acid together at high speed under vigorous mixing conditions by spraying the reactants through a two-phase, dual coaxial mixer/sprayer and separately controlling the supply and axial outflow rate of the phosphoric acid at 1 to 10 m/sec. and the outflow rate of ammonia at 200 to 1000 m/sec. (N.T.P.). Thorough mixing and a homogeneous product is obtained by directing the outflow spray into a coaxial cylindrical reaction chamber of a specified size with respect to the diameter of the outermost duct of the sprayer/mixer. The product may be granulated on a moving bed of granules and adjusted in respect of the NH.sub.3 to H.sub.3 PO.sub.4 content by changing the concentration of the phosphoric acid and/or supplying additional ammonia to the granulation bed.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.