Two-phase spraying device and reaction chamber for the preparation of a product containing ammonium orthophosphate
US4370304A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Aug 21, 1981 |
| Grant date | Jan 25, 1983 |
| Priority date | — |
| Expiry date | Aug 21, 2001 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY10S261/75
- WIPO fieldMaterials, metallurgy
- WIPO sectorChemistry
Abstract
Ammonium orthophosphate products are prepared by reacting ammonia and phosphoric acid together at high speed under vigorous mixing conditions by spraying the reactants through a two-phase, dual coaxial mixer/sprayer and separately controlling the supply and axial outflow rate of the phosphoric acid at 1 to 10 m/sec. and the outflow rate of ammonia at 200 to 1000 m/sec. (N.T.P.). Thorough mixing and a homogeneous product is obtained by directing the outflow spray into a coaxial cylindrical reaction chamber of a specified size with respect to the diameter of the outermost duct of the sprayer/mixer. The product may be granulated on a moving bed of granules and adjusted in respect of the NH.sub.3 to H.sub.3 PO.sub.4 content by changing the concentration of the phosphoric acid and/or supplying additional ammonia to the granulation bed.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.