Patent · US Expired

Distillative separations of gas mixtures containing methane, carbon dioxide and other components

US4462814A · kind A · utility

128Cited by
5References
32Claims
0Family size

Assignee

Inventors

Key dates

Filing dateMar 18, 1983
Grant dateJul 31, 1984
Priority date
Expiry dateMar 18, 2003

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10S62/929
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

Distillative separations of hydrocarbon feed mixtures containing at least methane and carbon dioxide, as well as other components, such as ethane, higher hydrocarbons, and hydrogen sulfide are disclosed. In the separations described, methane is preferably separated from an acid gas under conditions of composition, temperature and pressure which would normally produce acid gas solids. Acid gas solids are prevented by adding a liquid solids-preventing agent into this distillation column. A second distillation column is subsequently employed to further separate the feed gas mixture. The second distillation column is operated under conditions which an azeotrope would normally form between the light hydrocarbon and carbon dioxide, which azeotrope would limit the carbon dioxide overhead composition. The azeotrope is prevented by introducing an agent for preventing azeotrope formation. Alternatively, the second distillation column may be operated to separate carbon dioxide from hydrogen sulfide. In this case, a liquid agent is added to the second distillation column to increase the relative volatility of carbon dioxide to hydrogen sulfide. All liquid agents preferably comprise a C.sub.3 -…

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.