Preparation of low residual solvent content polyacrylonitrile filaments
US4505870A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Jun 17, 1983 |
| Grant date | Mar 19, 1985 |
| Priority date | — |
| Expiry date | Jun 17, 2003 |
Classification
- Technology area (CPC D)Textiles; Paper
- CPC primaryD01D5/04
- WIPO fieldTextile and paper machines
- WIPO sectorMechanical engineering
Abstract
Polyacrylonitrile filaments having a residual solvent content of less than 5% by weight and a total linear density of over 100,000 dtex can be prepared without contact with an extracting agent for the spinning solvent by a process in which PA0 (a) the spinning solution spun has a viscosity at 100.degree. C. of 10 to 60 falling-ball seconds, PA0 (b) the filaments are treated while still hot, directly at the end of the spinning cell, inside it or immediately outside the end of the cell, with a spin-finish which contains a lubricant and an antistat and which gives the filaments a moisture content of at most 10% by weight, relative to the solids content of the fibre, and PA0 (c) the filaments are immediately exposed to a heat treatment without cooling down first.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.