Method for the production of phenanthrenequinone
US4510090A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Jan 30, 1984 |
| Grant date | Apr 9, 1985 |
| Priority date | — |
| Expiry date | Jan 30, 2004 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07C2603/26
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
Improvement of the yield and purity of phenanthrenequinone during its production by oxidation of phenanthrene by means of chromic acid in a sulfuric acidic medium is achieved by preparing a dispersion made up of phenanthrene, alkali dichromate and water at 95.degree.-100.degree. C., cooling said dispersion down to 80.degree.-85.degree. C. and carrying out the oxidation reaction under cooling and portion-wise addition of concentrated sulfuric acid in a temperature range between 80.degree. and 85.degree. C.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.