Process for the preparation of stable aqueous solutions of water-soluble reactive dyes by membrane separation
US4523924A · kind A · utility
Assignee
Inventor
Key dates
| Filing date | Dec 12, 1983 |
| Grant date | Jun 18, 1985 |
| Priority date | — |
| Expiry date | Dec 12, 2003 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY10S8/918
- WIPO fieldBasic materials chemistry
- WIPO sectorChemistry
Abstract
The invention describes a process for the preparation of stable aqueous solutions of water-soluble reactive dyes, starting from an aqueous solution or suspension of the crude reactive dye which is concentrated and at least partially desalted by a membrane separation process. The process of the invention comprises continuously replacing part of the water which is drawn off from the dyestuff solution or suspension during the membrane separation process with demineralized water, whereby the concentration of calcium and magnesium ions in the dyestuff solution does not exceed 0.01% by weight. The concentrated and desalted dyestuff solution is stabilized by addition of a polyphosphate or dihydrogen phosphate/polyphosphate buffer, and a component which improves the water-solubility of the dye is optionally added. The formulations so obtained are readily storable for several months in the temperature range from -10.degree. to +40.degree. C.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.