Patent · US Expired

Biochemical process for optical resolution of cyclopentenolone derivatives

US4607013A · kind A · utility

15Cited by
1References
5Claims
0Family size

Assignee

Inventors

Key dates

Filing dateSep 7, 1984
Grant dateAug 19, 1986
Priority date
Expiry dateSep 7, 2004

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC12P7/26
  • WIPO fieldBiotechnology
  • WIPO sectorChemistry

Abstract

A biochemical process for optical resolution of 4-hydroxy-3-methyl-2-2'-propynyl-2-cyclopentenone, which comprises asymmetrically hydrolyzing organic carboxylic acid (saturated or unsaturated carboxylic acids having 1 to 18 carbon atoms) esters of (.+-.)-4-hydroxy-3-methyl-2-2'-propynyl-2-cyclopentenone by the action of an esterase originated from a microorganism or an animal pancreas to give optically active 4-hydroxy-3-methyl-2-2'-propynyl-2-cyclopentenone and esters of its antipode with high optical purity is disclosed. This resolution process is simple in steps as compared with the conventionally known organic chemical methods of optical resolution, and is quite advantageous industrially because it does not require expensive optically active reagents.

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