Patent · US Expired

Purification of tocopherols

US4617406A · kind A · utility

8Cited by
1References
8Claims
0Family size

Assignee

Inventor

Key dates

Filing dateFeb 11, 1985
Grant dateOct 14, 1986
Priority date
Expiry dateFeb 11, 2005

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07D311/72
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

Tocopherol homologues found in a tocopherol-containing feed material can be purified by forming a borate tocopherol ester and then distilling the material containing the esterified tocopherol to remove the materials boiling at temperatures lower than the esterified tocopherol. The borate tocopherol esters remaining after distillation are then reacted with a member selected from the group consisting of: Water, methanol, and ethanol to form tocopherol homologues from the borate tocopherol ester, and the boron by product from this reaction is removed. The tocopherol is then recovered by collecting it, distilling it or by any other convenient collection method.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.